Orgkhim Biochemical Holding Management Company, Joint Stock Company (orgkhim BCH Management Company, Jsc)

Russian Federation

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IPC Class
B01D 11/00 - Solvent extraction 1
B01D 11/04 - Solvent extraction of solutions which are liquid 1
C10C 3/08 - Working-up pitch, asphalt, bitumen by selective extraction 1
C10G 21/00 - Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents 1
C10G 21/02 - Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents with two or more solvents, which are introduced or withdrawn separately 1
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1.

Method for producing non-carcinogenic aromatic process oil

      
Application Number 14427798
Grant Number 09567532
Status In Force
Filing Date 2012-10-09
First Publication Date 2016-01-07
Grant Date 2017-02-14
Owner ORGKHIM BIOCHEMICAL HOLDING MANAGEMENT COMPANY, JOINT STOCK COMPANY (ORGKHIM BCH MANAGEMENT COMPANY, JSC) (Russia)
Inventor
  • Tsebulaev, Victor Alekseevich
  • Khodov, Nikolay Vladimirovich
  • Kuimov, Andrey Fedorovich
  • Radbil, Arkadiy Benyuminovich
  • Dolinskiy, Taras Ivanovich
  • Mazurin, Oleg Anatolyevich

Abstract

The present invention relates to the chemical or petroleum-processing industry and can be used in the production of petroleum plasticizers for synthetic rubber and tyres. In the method for producing non-carcinogenic aromatic process oil, containing a PCA extract of less than 3.0% according to the IP-346 method, said method comprising purifying the oil fractions of petroleum with selective solvents and separating the extract, additionally processing the extract with a polar solvent and producing a raffinate as the end product, the polar solvent used is a mixture of dimethylsulphoxide and Nmethylpyrrolidone, which is used for preliminary processing of the extract, wherein, after the preliminary processing, the mixture of extract and polar solvent is filtered, divided and the light phase is sent to the additional processing of the extract with the polar solvent, and the heavy phase is sent to a polar solvent regeneration stage. The ratio of dimethylsulphoxide to N-methylpyrrolidone in the mixture is within the range of 1:0.1-0.5. The ratio of polar solvent to extract in the additional processing stage is within the range of 1.5-2.5:1. The ratio of polar solvent to extract in the preliminary processing stage is within the range of 0.1-0.3:1. The technical result consists in increasing the efficiency of the process by preventing the formation of an intermediate layer in the extractor column, by reducing the ratio of solvent:extract, and, as a consequence, by increasing the productivity of the plant, simplifying the process of drying the solvent, and eliminating a paraffin-naphthene solvent, which substantially simplifies the regeneration of extractant from the raffinate solution.

IPC Classes  ?

  • C10G 21/12 - Organic compounds only
  • C10G 21/20 - Nitrogen-containing compounds
  • C10G 21/22 - Compounds containing sulfur, selenium, or tellurium
  • C10G 29/28 - Organic compounds not containing metal atoms containing sulfur as the only hetero atom, e.g. mercaptans, or sulfur and oxygen as the only hetero atoms
  • C10G 21/16 - Oxygen-containing compounds
  • C10G 21/28 - Recovery of used solvent
  • C10G 21/02 - Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents with two or more solvents, which are introduced or withdrawn separately
  • C10G 29/20 - Organic compounds not containing metal atoms
  • C10G 21/00 - Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
  • B01D 11/00 - Solvent extraction
  • B01D 11/04 - Solvent extraction of solutions which are liquid
  • C10C 3/08 - Working-up pitch, asphalt, bitumen by selective extraction